Water and sediment chemistry data were collected over the summer and fall of 2017 at Second Creek, a riparian wetland study site near Aurora, MN, to understand sulfur and methane processes. Porewaters were collected with two distinct methods “peepers” (multi-chambered equilibrium dialysis samplers) that allow for high vertical resolution but 2-3 week averaged temporal resolution, and rhizon samplers that enable instantaneous temporal resolution but have lower spatial resolution. Porewaters were analyzed for dissolved cations, anions, sulfide, methane, iron(II)/iron(III), and pH. Sediment cores were analyzed for acid volatile sulfide, and sulfur and iron speciation via X-ray absorption spectroscopy.